Title: Amplifying Solventless Synthesis: One-pot Multistep Mechanochemical Synthesis of Fluorinated Pyrazolones

Citation
Howard JL, Nicholson W, Sagatov Y, et al. (2017). Amplifying Solventless Synthesis: One-pot Multistep Mechanochemical Synthesis of Fluorinated Pyrazolones. Cardiff University. http://doi.org/10.17035/d.2017.0038572887


Access Rights: Data can be made freely available subject to attribution
Access Method: Click to email a request for this data to opendata@cardiff.ac.uk

Cardiff University Dataset Creators

Dataset Details
Publisher: Cardiff University
Date (year) of data becoming publicly available: 2017
Data format: txt, .inmr, .info, .par, .xml, .pdf, .temp, .back, .jpg, .ispd
Software Required: An appropriate NMR processing software is required for raw NMR data files
Estimated total storage size of dataset: Less than 100 megabytes
DOI: 10.17035/d.2017.0038572887

Description
A one-pot, two step mechanochemical synthesis process has been developed, of fluorinated pyrazolones. The experiments here have provided a logical approach to multistep solventless synthesis under milling conditions. This demonstrates the applicability of mechanochemical synthesis to multistep procedures.

Analysis of reaction products from this methodology resulted in the following data:
1H, 19F and 13C NMR raw data files
IR spectra
High-Resolution Mass Spectrography spectra.

Research results based upon these data are published as http://doi.org/10.3762/bjoc.13.189

Keywords

Mechanochemistry

Related Projects

Last updated on 2018-08-10 at 11:23