Teitl: Amplifying Solventless Synthesis: One-pot Multistep Mechanochemical Synthesis of Fluorinated Pyrazolones

Dyfyniad
Howard JL, Nicholson W, Sagatov Y, et al. (2017). Amplifying Solventless Synthesis: One-pot Multistep Mechanochemical Synthesis of Fluorinated Pyrazolones. Cardiff University. http://doi.org/10.17035/d.2017.0038572887


Hawliau Mynediad: Gall data fod ar gael yn rhad ac am ddim yn amodol ar briodoli
Dull Mynediad: I anfon cais i gael y data hwn, ebostiwch opendata@caerdydd.ac.uk

Crewyr y Set Ddata o Brifysgol Caerdydd

Manylion y Set Ddata
Cyhoeddwr: Cardiff University
Dyddiad (y flwyddyn) pryd y daeth y data ar gael i'r cyhoedd: 2017
Fformat y data: txt, .inmr, .info, .par, .xml, .pdf, .temp, .back, .jpg, .ispd
Meddalwedd ofynnol: An appropriate NMR processing software is required for raw NMR data files
Amcangyfrif o gyfanswm maint storio'r set ddata: Llai na 100 megabeit
DOI: 10.17035/d.2017.0038572887

Disgrifiad
A one-pot, two step mechanochemical synthesis process has been developed, of fluorinated pyrazolones. The experiments here have provided a logical approach to multistep solventless synthesis under milling conditions. This demonstrates the applicability of mechanochemical synthesis to multistep procedures.

Analysis of reaction products from this methodology resulted in the following data:
1H, 19F and 13C NMR raw data files
IR spectra
High-Resolution Mass Spectrography spectra.

Research results based upon these data are published as http://doi.org/10.3762/bjoc.13.189

Allweddeiriau

Mechanochemistry

Prosiectau Cysylltiedig

Diweddarwyd y tro diwethaf ar 2018-08-10 am 11:23