Teitl: A Ball-Milling Enabled Reformatsky Reaction

Dyfyniad
Cao Q, Stark RT, Fallis IA, et al. (2019). A Ball-Milling Enabled Reformatsky Reaction. Cardiff University. http://doi.org/10.17035/d.2019.0075438608


Hawliau Mynediad: Darperir Data dan drwydded Creative Commons Attribution (CC BY 4.0)
Dull Mynediad: I anfon cais i gael y data hwn, ebostiwch opendata@caerdydd.ac.uk

Crewyr y Set Ddata o Brifysgol Caerdydd

Manylion y Set Ddata
Cyhoeddwr: Cardiff University
Dyddiad (y flwyddyn) pryd y daeth y data ar gael i'r cyhoedd: 2019
Dyddiad dechrau creu'r data: 01.06.2017
Dyddiad gorffen creu'r data: 05.01.2019
Fformat y data: .jpg .fid
Meddalwedd ofynnol: .fid files are processed using standard NMR processing software.
DOI: 10.17035/d.2019.0075438608

Disgrifiad

The data here contains a selection of 1H, 13C, 19F NMR data, as well as IR, MS and any relevant chromatography information. Some files may be processed in advance and deposited and some may require access to typical processing tools for data of this type.
Abstract: An operationally simple one‐jar one‐step mechanochemical Reformatsky reaction using in situ generated organozinc intermediates under neat grinding conditions has been developed. Notable features are that this reaction protocol requires no solvent, no inert gases and no pre‐activation of the bulk zinc source. The developed process is demonstrated to have good substrate scope (39‐82% yield), and is effective irrespective of the morphology of the zinc source.

Research results based upone these data are published at http://doi.org/10.1002/cssc.201900886



Allweddeiriau

Mechanochemistry, Organozinc

Prosiectau Cysylltiedig

Diweddarwyd y tro diwethaf ar 2019-21-06 am 10:20