Teitl: Manganese-Catalyzed One-Pot Conversion of Nitroarenes into N-Methylarylamines Using Methanol - data

Dyfyniad
Reed-Berendt B, Mast N, Morrill LC (2020). Manganese-Catalyzed One-Pot Conversion of Nitroarenes into N-Methylarylamines Using Methanol - data. Cardiff University. http://doi.org/10.17035/d.2020.0098190202


Hawliau Mynediad: Darperir Data dan drwydded Creative Commons Attribution (CC BY 4.0)
Dull Mynediad: I anfon cais i gael y data hwn, ebostiwch opendata@caerdydd.ac.uk

Crewyr y Set Ddata o Brifysgol Caerdydd

Manylion y Set Ddata
Cyhoeddwr: Cardiff University
Dyddiad (y flwyddyn) pryd y daeth y data ar gael i'r cyhoedd: 2020
Fformat y data: .txt, .inmr, .info, .par, .xml, .pdf, .temp, .back, .jpg, .ispd
Meddalwedd ofynnol: An appropriate NMR processing software is required for raw NMR data files
Amcangyfrif o gyfanswm maint storio'r set ddata: Llai na 100 megabeit
Nifer y ffeiliau yn y set ddata: 1225
DOI: 10.17035/d.2020.0098190202

Disgrifiad

A manganese-catalyzed one-pot conversion of nitroarenes into N-methylarylamines has been developed. This transfer hydrogenation method employs a well-defined bench stable Mn PN3P pincer precatalyst in combination with methanol as both the reductant and the C1 source. A selection of commercially available nitroarenes was converted into N-methylarylamines in synthetically useful yields.

Analysis of reaction products from this methodology resulted in the following data:

1H, 19F and 13C NMR raw data files

IR spectra

High resolution mass spectrometry spectra.    

Research results based upon these data are published at http://doi.org/10.1002/ejoc.201901854


Prosiectau Cysylltiedig
Homogeneous hydrogen transfer catalysis (01.10.2016 - 30.09.2019)

Diweddarwyd y tro diwethaf ar 2020-26-06 am 10:47